ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

Base Information

Chemical Name:ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)
CAS No.:640721-17-1
Molecular Formula:C₃₉H₃₅ClFeOP₂Ru
Molecular Weight:774.024
Hs Code.:

Synonyms:ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

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Chemical Property of ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

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Technology Process of ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

There total 1 articles about ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 114925-38-1
(η3-2-methylallyl)Ru(CO)3Cl

: 640721-17-1
ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

Guidance literature:: In tetrahydrofuran; N2; adding 1 equiv. of diphosphine to THF soln. of Ru complex at room temp., refluxing for 7 h; evapn. to dryness, dissolving the residue in CH2Cl2, chromy. (neutral Al2O3, methanol), solvent removal; elem. anal.;
DOI:10.1021/om030530e

Reference yield: 97.0%

: 26042-64-8
silver hexafluoroantimonate

: 640721-17-1
ruthenium(II)(η3-2-C3H4Me)(CO)Cl(1,1'bis(diphenylphosphino)ferrocene)

: 828917-23-3
[Ru(η3-2-C3H4Me)(CO)(1,1'-bis(diphenylphosphino)ferrocene)][SbF6]

Guidance literature:: In dichloromethane; byproducts: AgCl; Ru complex in CH2Cl2 treated with 1 equiv. of Ag salt, stirred for 15 min at room temp. (absence of light); filtered, evapd., washed (diethyl ether), dried (vac.), elem. anal.;
DOI:10.1039/b410812d