1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

Base Information

Chemical Name:1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate
CAS No.:1615250-67-3
Molecular Formula:C₁₈H₂₈N₄O₄
Molecular Weight:364.445
Hs Code.:

Synonyms:1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

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Chemical Property of 1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

Chemical Property:

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Technology Process of 1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

There total 3 articles about 1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1319730-89-6
2-(N-(tert-butoxycarbonyl)thioureido)ethyl acetate

: 5840-09-5
4-amino-1-(N-ethylamino)benzene

: 1615250-67-3
1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 1319730-88-5
N-tert-butoxycarbonyl-N’-(2-hydroxyethyl)thiourea

: 1615250-67-3
1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 3 h / 0 - 20 °C

2: mercury dichloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C

With pyridine; dmap; triethylamine; mercury dichloride; In dichloromethane;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1615250-67-3
1-[1-(tert-butoxycarbonyl)-3-(4-ethylaminophenyl)guanidino]ethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.75 h / 0 - 20 °C / Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

2.1: pyridine; dmap / dichloromethane / 3 h / 0 - 20 °C

3.1: mercury dichloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C

With pyridine; dmap; sodium hydride; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057