4-Methyl-2-nitropyridin-3-ol

Base Information

Chemical Name:4-Methyl-2-nitropyridin-3-ol
CAS No.:15128-89-9
Molecular Formula:C₆H₆N₂O₃
Molecular Weight:154.125
Hs Code.:2933399090
DSSTox Substance ID:DTXSID30552082
Wikidata:Q82432076
Mol file:15128-89-9.mol

Synonyms:4-Methyl-2-nitropyridin-3-ol;15128-89-9;3-Hydroxy-4-methyl-2-nitropyridine;3-Pyridinol, 4-methyl-2-nitro-;4-Methyl-2-nitro-3-pyridinol;MFCD16556274;3-hydroxy-4-methyl-2-nitro pyridine;SCHEMBL1807427;DTXSID30552082;COIBQJMOZNXKIB-UHFFFAOYSA-N;AKOS016007477;SB52447;AC-33883;CS-12599;SY107602;CS-0102095;EN300-332043;F51133;A884096;Z1255452532

Suppliers and Price of 4-Methyl-2-nitropyridin-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methyl-2-nitropyridin-3-ol
100mg
$ 220.00

Labseeker
3-hydroxy-4-methyl-2-nitropyridine 95
250g
$ 7000.00

Crysdot
4-Methyl-2-nitropyridin-3-ol 95+%
1g
$ 279.00

Crysdot
4-Methyl-2-nitropyridin-3-ol 95+%
10g
$ 1493.00

Crysdot
4-Methyl-2-nitropyridin-3-ol 95+%
5g
$ 830.00

ChemScene
4-Methyl-2-nitropyridin-3-ol ≥97.0%
100mg
$ 70.00

ChemScene
4-Methyl-2-nitropyridin-3-ol ≥97.0%
250mg
$ 115.00

ChemScene
4-Methyl-2-nitropyridin-3-ol ≥97.0%
5g
$ 798.00

ChemScene
4-Methyl-2-nitropyridin-3-ol ≥97.0%
1g
$ 260.00

Chemenu
4-Methyl-2-nitropyridin-3-ol 95%
1g
$ 421.00

Total 20 raw suppliers

Chemical Property of 4-Methyl-2-nitropyridin-3-ol

Chemical Property:

Boiling Point:389.8±37.0 °C(Predicted)
PKA:0.95±0.30(Predicted)
PSA：78.94000
Density:1.411±0.06 g/cm3(Predicted)
LogP:1.52700
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:154.03784206
Heavy Atom Count:11
Complexity:156

Purity/Quality:

99%, ^*data from raw suppliers

4-Methyl-2-nitropyridin-3-ol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=NC=C1)[N+](=O)[O-])O

Technology Process of 4-Methyl-2-nitropyridin-3-ol

There total 7 articles about 4-Methyl-2-nitropyridin-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1121-19-3
4-methylpyridin-3-ol

: 15128-89-9
2-nitro-3-hydroxy-4-methylpyridine

Guidance literature:: With sulfuric acid; nitric acid; at 0 - 40 ℃; for 2.75h;

Reference yield:

: 15128-89-9
2-nitro-3-hydroxy-4-methylpyridine

Guidance literature:: With sulfuric acid; at 0 - 5 ℃;
DOI:10.1021/jo01265a121

Reference yield:

: 1003-67-4
4-methylpyridine-1-oxide

: 15128-89-9
2-nitro-3-hydroxy-4-methylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2 h / Reflux

2.1: potassium hydroxide / methanol / 20 °C

2.2: pH 7

3.1: nitric acid; sulfuric acid / 2 h / 10 - 20 °C

3.2: pH 2

With sulfuric acid; nitric acid; potassium hydroxide; In methanol;