dimethyl(o-tolyl)chlorosilane

Base Information

• Chemical Name: dimethyl(o-tolyl)chlorosilane
• CAS No.: 17146-06-4
• Molecular Formula: C₉H₁₃ClSi
• Molecular Weight: 184.741
• Mol file: 17146-06-4.mol

Synonyms:dimethyl(o-tolyl)chlorosilane

Chemical Property of dimethyl(o-tolyl)chlorosilane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of dimethyl(o-tolyl)chlorosilane

There total 7 articles about dimethyl(o-tolyl)chlorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

dimethylsilicon dichloride (75-78-5,30107-43-8) + 2-methylphenylboronic acid pinacol ester (195062-59-0) → dimethyl(o-tolyl)chlorosilane (17146-06-4) + Dimethyl-bis-(o-tolyl)-silan (19420-76-9)

Guidance literature:

2-methylphenylboronic acid pinacol ester; With bis(tricyclohexylphosphine)nickel(II) dichloride; triethylaluminum; dimethylaluminum chloride; In 1,4-dioxane; hexane; 1,3,5-trimethyl-benzene; at 90 ℃; for 0.5h;

dimethylsilicon dichloride; In hexane; toluene; 1,3,5-trimethyl-benzene; at 90 ℃; for 24h;

Reference yield: 15.0%

chloromethyldimethylphenylsilane (1833-51-8) → dimethyl(o-tolyl)chlorosilane (17146-06-4)

Guidance literature:

aluminium trichloride; at 90 ℃; for 0.0833333h;

Reference yield: 13.0%

1,2-dichlorotetramethylsilane (4342-61-4) + ortho-toluoyl chloride (933-88-0) → dimethyl(o-tolyl)chlorosilane (17146-06-4)

Guidance literature:

bis(benzonitrile)palladium(II) dichloride; triphenylphosphine; at 145 ℃; for 15h;

DOI:10.1021/ja00197a058

upstream raw materials:

2-methylphenyl bromide

dimethylsilicon dichloride

chloromethyldimethylphenylsilane

1,2-dichlorotetramethylsilane

Downstream raw materials:

dimethyl(2-methylphenyl)methoxysilane

(3-chloroprop-1-ynyl)dimethyl(o-tolyl)silane

(R)-methyl 4-(4-(dimethyl(o-tolyl)silyl)-1-hydroxybut-3-ynyl)benzoate

C₂₈H₃₉LiSi₃