meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Base Information

Chemical Name:meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine
CAS No.:58519-82-7
Molecular Formula:C₃₀H₂₈N₂O₄
Molecular Weight:480.563
Hs Code.:

Synonyms:meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Suppliers and Price of meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Chemical Property:

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Technology Process of meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

There total 5 articles about meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 51208-45-8,119386-71-9,870991-68-7,870991-70-1
meso-1,2-Bis-(2-hydroxyphenyl)ethylenediamine

: 135-02-4
ortho-anisaldehyde

: 58519-82-7
meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Guidance literature:: In acetonitrile; for 3h; Heating;
DOI:10.1016/0223-5234(93)90003-W

Reference yield:

: 58520-46-0,148240-65-7,149949-25-7
N,N'-(1,2-bis(2-methoxyphenyl)ethane-1,2-diyl)dibenzamide

: 58519-82-7
meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: BBr₃ / CH₂Cl₂ / a) -60 deg C, 30 min, b) 3 d, RT

2: 87 percent / acetonitrile / 3 h / Heating

With boron tribromide; In dichloromethane; acetonitrile;
DOI:10.1016/0223-5234(93)90003-W

Reference yield:

: meso-N,N'-bis(2-methoxybenzylidene)1,2-bis(2-methoxyphenyl)ethylenediamine

: 58519-82-7
meso-N,N'-bis(2-hydroxybenzyliden)1,2-bis(2-methoxyphenyl)ethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 6 N aq. H₂SO₄

2: BBr₃ / CH₂Cl₂ / a) -60 deg C, 30 min, b) 3 d, RT

3: 87 percent / acetonitrile / 3 h / Heating

With sulfuric acid; boron tribromide; In dichloromethane; acetonitrile;
DOI:10.1016/0223-5234(93)90003-W