Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

Base Information

Chemical Name:Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate
CAS No.:263754-54-7
Molecular Formula:C₂₀H₂₀O₃
Molecular Weight:308.377
Hs Code.:

Synonyms:Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

Suppliers and Price of Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

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Technology Process of Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

There total 4 articles about Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 74-88-4
methyl iodide

: 263753-02-2
(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoic acid

: 263754-54-7
Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2004.11.051

Reference yield:

: 263753-02-2
(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoic acid

: 263754-54-7
Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

Guidance literature:: With NaH; methyl iodide; In N,N-dimethyl-formamide;

Reference yield:

: 3354-58-3
2-allyl-6-methylphenol

: 263754-54-7
Methyl(E)-3-(2-((E)-3-(2-hydroxy-3-methylphenyl)-2-propenyl)phenyl)-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / Pd(OAc)2; LiCl; LiOAc / Bu₄NCl / dimethylformamide / 16 h / 100 °C

2: 94 percent / NaH / dimethylformamide / 2 h / 20 °C

With palladium diacetate; lithium acetate; sodium hydride; lithium chloride; tetrabutyl-ammonium chloride; In N,N-dimethyl-formamide; 1: Heck reaction;
DOI:10.1016/j.bmcl.2004.11.051