4'-O-benzyl-α-hydroxyacetosyringone

Base Information

• Chemical Name: 4'-O-benzyl-α-hydroxyacetosyringone
• CAS No.: 873978-83-7
• Molecular Formula: C₁₇H₁₈O₅
• Molecular Weight: 302.327
• Mol file: 873978-83-7.mol

Synonyms:4'-O-benzyl-α-hydroxyacetosyringone

Chemical Property of 4'-O-benzyl-α-hydroxyacetosyringone

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-O-benzyl-α-hydroxyacetosyringone

There total 5 articles about 4'-O-benzyl-α-hydroxyacetosyringone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloride (100-44-7) → 4'-O-benzyl-α-hydroxyacetosyringone (873978-83-7)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / 8 h / 20 °C

2: 60 percent / t-BuOK

3: 10 percent / 10 percent HCl / 5 h / Heating

With hydrogenchloride; potassium tert-butylate; In methanol;

DOI:10.3390/51201287

Reference yield:

syringic aldehyde (134-96-3) → 4'-O-benzyl-α-hydroxyacetosyringone (873978-83-7)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / 8 h / 20 °C

2: 60 percent / t-BuOK

3: 10 percent / 10 percent HCl / 5 h / Heating

With hydrogenchloride; potassium tert-butylate; In methanol;

DOI:10.3390/51201287

Reference yield:

4-(benzyloxy)-3,5-dimethoxybenzaldehyde (6527-32-8) → 4'-O-benzyl-α-hydroxyacetosyringone (873978-83-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / t-BuOK

2: 10 percent / 10 percent HCl / 5 h / Heating

With hydrogenchloride; potassium tert-butylate;

DOI:10.3390/51201287

upstream raw materials:

dibenzoyl peroxide

4-(benzyloxy)-3,5-dimethoxybenzaldehyde

benzyl chloride

syringic aldehyde

Downstream raw materials:

3',5'-dimethoxy-4'-hydroxy-(2-hydroxy)acetophenone