2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Base Information

Chemical Name:2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid
CAS No.:75863-51-3
Molecular Formula:C₃₂H₂₆N₂O₁₀
Molecular Weight:598.566
Hs Code.:

Synonyms:2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Suppliers and Price of 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

There total 5 articles about 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75863-50-2
benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

: 75863-51-3
2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; Ambient temperature;
DOI:10.1021/jo00316a021

Reference yield:

: 75917-52-1
ethyl 1,5,6-trideoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-ribo-hept-5-enofuranuronate

: 75863-51-3
2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂ / PtO₂ / ethanol / 20 h / 2482.3 Torr / Ambient temperature

2: 1.) 1 N H₂SO₄; 2.) 50percent NaOH / 1.) 60 deg C, 1 h; 2.) ambient temp. 20 h

3: 1.) SOCl₂

4: 98 percent / pyridine / ice bath 1 h, ambient temp. 40 h

5: 90 percent / H₂ / Pd/C / acetic acid / Ambient temperature

With sodium hydroxide; thionyl chloride; sulfuric acid; hydrogen; platinum(IV) oxide; palladium on activated charcoal; In pyridine; ethanol; acetic acid;
DOI:10.1021/jo00316a021

Reference yield:

: 65926-38-7
1,5,6-trideoxy-1-(uracil-1-yl)-β-D-ribo-heptofuranuronic acid

: 75863-51-3
2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptafuranuronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) SOCl₂

2: 98 percent / pyridine / ice bath 1 h, ambient temp. 40 h

3: 90 percent / H₂ / Pd/C / acetic acid / Ambient temperature

With thionyl chloride; hydrogen; palladium on activated charcoal; In pyridine; acetic acid;
DOI:10.1021/jo00316a021