benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

Base Information

Chemical Name:benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate
CAS No.:75863-50-2
Molecular Formula:C₃₉H₃₂N₂O₁₀
Molecular Weight:688.69
Hs Code.:

Synonyms:benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

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Chemical Property of benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

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Technology Process of benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

There total 4 articles about benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 75863-49-9
benzyl-1,5,6-trideoxy-1-(uracil-1-yl)-β-D-ribo-heptofuranuronate

: 98-88-4
benzoyl chloride

: 75863-50-2
benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

Guidance literature:: In pyridine; ice bath 1 h, ambient temp. 40 h;
DOI:10.1021/jo00316a021

Reference yield:

: 75917-52-1
ethyl 1,5,6-trideoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-ribo-hept-5-enofuranuronate

: 75863-50-2
benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / PtO₂ / ethanol / 20 h / 2482.3 Torr / Ambient temperature

2: 1.) 1 N H₂SO₄; 2.) 50percent NaOH / 1.) 60 deg C, 1 h; 2.) ambient temp. 20 h

3: 1.) SOCl₂

4: 98 percent / pyridine / ice bath 1 h, ambient temp. 40 h

With sodium hydroxide; thionyl chloride; sulfuric acid; hydrogen; platinum(IV) oxide; In pyridine; ethanol;
DOI:10.1021/jo00316a021

Reference yield:

: 75863-48-8
ethyl 1,5,6-trideoxy-2,3-O-isopropylidene-1-(uracil-1-yl)-β-D-ribo-heptofuranuronate

: 75863-50-2
benzyl 2,3-di-O-benzoyl-1-(3-benzoyluracil-1-yl)-1,5,6-trideoxy-β-D-ribo-heptofuranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1 N H₂SO₄; 2.) 50percent NaOH / 1.) 60 deg C, 1 h; 2.) ambient temp. 20 h

2: 1.) SOCl₂

3: 98 percent / pyridine / ice bath 1 h, ambient temp. 40 h

With sodium hydroxide; thionyl chloride; sulfuric acid; In pyridine;
DOI:10.1021/jo00316a021