Ru(SC₆H₄P(C₆H₅)2)3CH₂CH

Base Information

• Chemical Name: Ru(SC₆H₄P(C₆H₅)2)3CH₂CH
• CAS No.: 1383842-29-2
• Molecular Formula: C₅₆H₄₅P₃RuS₃
• Molecular Weight: 1008.16

Synonyms:Ru(SC₆H₄P(C₆H₅)2)3CH₂CH

Chemical Property of Ru(SC₆H₄P(C₆H₅)2)3CH₂CH

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Technology Process of Ru(SC₆H₄P(C₆H₅)2)3CH₂CH

There total 1 articles about Ru(SC₆H₄P(C₆H₅)2)3CH₂CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Ru(SC6H4P(C6H5)2)3CH2CH2(1+)*PF6(1-)=Ru(SC6H4P(C6H5)2)3CH2CH2PF6 (952064-97-0) → Ru(SC6H4P(C6H5)2)3CH2CH (1383842-29-2)

Guidance literature:

With KOH; In methanol; acetonitrile; (under N2 or Ar, Schlenk); MeOH soln. of KOH added to soln. of Ru-complex in MeCN, stirred for 30 min; solvent removed by rotary evapn., washed with H2O; elem. anal.;

DOI:10.1021/ic300983x

Reference yield: 90.0%

Ru(SC6H4P(C6H5)2)3CH2CH (1383842-29-2) + hydrogen chloride (7698-05-7) → Ru(SC6H4P(C6H5)2)3CH2CH(2)H(1+)*Cl(1-)=Ru(SC6H4P(C6H5)2)3CH2CH(2)HCl

Guidance literature:

In water-d2; benzene; (under N2 or Ar, Schlenk); soln. of DCl in D2O added to soln. of Ru-complex in benzene, refluxed for 1 h; solvent removed by rotary evapn., washed with H2O, Et2O;

DOI:10.1021/ic300983x

upstream raw materials:

Ru(SC₆H₄P(C₆H₅)2)3CH₂CH₂⁽¹⁺⁾*PF₆^(1-)=Ru(SC₆H₄P(C₆H₅)2)3CH₂CH₂PF₆

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