(R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

Base Information

Chemical Name:(R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate
CAS No.:1531624-40-4
Molecular Formula:C₂₀H₂₀O₄
Molecular Weight:324.376
Hs Code.:

Synonyms:(R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

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Chemical Property of (R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

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Technology Process of (R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

There total 2 articles about (R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1531624-21-1
6-tert-butyl-3-methylbenzofuran-2-yl phenyl carbonate

: 1531624-40-4
(R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

: (S)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

Guidance literature:: With (R)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazol-7-yl acetate; In tert-Amyl alcohol; at 0 ℃; for 36h; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1039/c3cc47455k

Reference yield:

: 173419-97-1
6-(tert-butyl)-3-methylbenzofuran-2(3H)-one

: 1885-14-9
phenyl chloroformate

: 1531624-40-4
(R)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

: (S)-phenyl 6-tert-butyl-3-methyl-2-oxo-2,3-dihydrobenzofuran-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / Inert atmosphere

2: (R)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazol-7-yl acetate / tert-Amyl alcohol / 36 h / 0 °C / Inert atmosphere; Molecular sieve

With (R)-6,7-dihydro-5H-pyrrolo[1,2-a]imidazol-7-yl acetate; triethylamine; In tetrahydrofuran; tert-Amyl alcohol;
DOI:10.1039/c3cc47455k