1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Base Information

Chemical Name:1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol
CAS No.:81712-83-6
Molecular Formula:C₁₇H₂₄O₉S
Molecular Weight:404.438
Hs Code.:

Synonyms:1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Suppliers and Price of 1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

There total 6 articles about 1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 81712-82-5
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

: 81712-83-6
1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane; acetic acid; for 0.333333h; Ambient temperature;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-81-4
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,6-O-isopropyliden-chiro-inositol

: 81712-83-6
1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / 20 h / 60 °C

2: 94 percent / hydrogen / 10 percent palladium-carbon / dioxane; acetic acid / 0.33 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In 1,4-dioxane; acetic acid;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-79-0
1L-7-O-Benzoyl-2,3,4-tri-O-benzyl-1-C-hydroxymethyl-chiro-inositol

: 81712-83-6
1L-1-C-Hydroxymethyl-5,6-O-isopropyliden-7-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) p-toluene-sulphonic acid; 2.) triethylamine / 1.) THF, 4 h, 70 deg C

2: sodium methoxide / methanol / 20 h / Ambient temperature

3: 81 percent / pyridine / 20 h / 60 °C

4: 94 percent / hydrogen / 10 percent palladium-carbon / dioxane; acetic acid / 0.33 h / Ambient temperature

With pyridine; hydrogen; sodium methylate; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; acetic acid;
DOI:10.1016/S0008-6215(00)88052-0