2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide

Base Information

• Chemical Name: 2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide
• CAS No.: 1365619-38-0
• Molecular Formula: C₂₈H₂₉FN₆O₄
• Molecular Weight: 532.574

Synonyms:2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide

Chemical Property of 2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide

Chemical Property:

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Technology Process of 2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide

There total 1 articles about 2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

O6-(benzotriazol-1-yl)-2-fluoro-2',3'-O-isopropylideneinosine-5'-N-methylcarboxamide (1277176-28-9) + 2,2-Diphenylethylamine (3963-62-0) → 2-fluoro-N(6)-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide (1365619-38-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 25 ℃; for 16h;

DOI:10.1021/jm300206u

Reference yield: 74.0%

2-(4-N-(3,5-di-tert-butyl-4-hydroxyphenylcarboxy)aminophenyl)ethylamine (1365619-25-5) + 2-fluoro-N(6)-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide (1365619-38-0) → C51H60N8O6 (1365619-44-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 150 ℃; for 2h;

DOI:10.1021/jm300206u

Reference yield: 40.0%

2-fluoro-N(6)-(2,2-diphenylethyl)-2',3'-O-isopropylideneadenosine-5'-N-methylcarboxamide (1365619-38-0) → 2-fluoro-N(6)-(2,2-diphenylethyl)adenosine-5'-N-methylcarboxamide (1365619-40-4)

Guidance literature:

With hydrogenchloride; water; In acetonitrile; at 50 ℃; for 2h;

DOI:10.1021/jm300206u

upstream raw materials:

O⁶-(benzotriazol-1-yl)-2-fluoro-2',3'-O-isopropylideneinosine-5'-N-methylcarboxamide

2,2-Diphenylethylamine

Downstream raw materials:

C₅₁H₆₀N₈O₆

2-(2-(4-N-(3,5-di-tert-butyl-4-hydroxyphenylcarboxy)aminophenyl))ethylamino-N⁽⁶⁾-(2,2-diphenylethyl)adenosine-5'-N-methylcarboxamide

2-fluoro-N⁽⁶⁾-(2,2-diphenylethyl)adenosine-5'-N-methylcarboxamide

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