benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

Base Information

Chemical Name:benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate
CAS No.:1357928-67-6
Molecular Formula:C₂₃H₂₈ClN₅O₄
Molecular Weight:473.959
Hs Code.:

Synonyms:benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

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Chemical Property of benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

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Technology Process of benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

There total 2 articles about benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 99616-43-0
3-(benzyloxy)-3-oxopropan-1-aminium chloride

: 150824-47-8
nitenpiram

: 1357928-67-6
benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

Guidance literature:: With triethylamine; In ethanol; at 65 ℃; for 0.416667h; Microwave irradiation;
DOI:10.1002/jhet.1558

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1357928-67-6
benzyl 3-[4-[N-((6-chloro-3-pyridyl)methyl)-N-ethyl]amino-3-methyl-5-nitro-1,2,3,6-tetrahydropyrimidin-1-yl]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 80 °C

2: triethylamine / ethanol / 0.42 h / 65 °C / Microwave irradiation

With thionyl chloride; triethylamine; In ethanol; 2: |Mannich Aminomethylation;
DOI:10.1002/jhet.1558