3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

Base Information

Chemical Name:3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide
CAS No.:182923-92-8
Molecular Formula:C₂₈H₂₆N₄O₇
Molecular Weight:530.537
Hs Code.:

Synonyms:3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

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Chemical Property of 3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

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Technology Process of 3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

There total 15 articles about 3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 182923-89-3
Chloro-acetic acid (2R,3S,4R,5R,6R)-6-azido-4-benzyloxy-5-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(4-methoxy-phenoxymethyl)-tetrahydro-pyran-3-yl ester

: 182923-92-8
3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

Guidance literature:: With potassium carbonate; In methanol; dichloromethane;
DOI:10.1016/0040-4039(96)01394-9

Reference yield: 88.9%

: 1404438-26-1
C₂₂H₁₉F₃N₄O₈S

: 150-76-5
4-methoxy-phenol

: 182923-92-8
3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

Guidance literature:: With Aliquat 336; sodium hydroxide; In dichloromethane; water; at -80 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.201200468

Reference yield:

: 150-76-5
4-methoxy-phenol

: 182923-92-8
3-O-benzyl-2-deoxy-6-O-(p-methoxyphenyl)-2-phthalimido-β-D-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / DEAD, Ph₃P / CH₂Cl₂ / 0 °C

2: 97 percent / pyridine / CH₂Cl₂ / 0 °C

3: 91 percent / TMS-N₃, BF₃*Et₂O, mol. sieves 4 Angstroem / CH₂Cl₂

4: 96 percent / K₂CO₃ / methanol; CH₂Cl₂

With pyridine; trimethylsilylazide; 4 A molecular sieve; boron trifluoride diethyl etherate; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In methanol; dichloromethane;
DOI:10.1016/0040-4039(96)01394-9