C₂₇H₃₆O₃

Base Information

Chemical Name:C₂₇H₃₆O₃
CAS No.:944913-72-8
Molecular Formula:C₂₇H₃₆O₃
Molecular Weight:408.581
Hs Code.:

C<sub>27</sub>H<sub>36</sub>O<sub>3</sub>

Synonyms:C₂₇H₃₆O₃

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Chemical Property of C₂₇H₃₆O₃

Chemical Property:

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Technology Process of C₂₇H₃₆O₃

There total 8 articles about C₂₇H₃₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 944913-71-7
C₃₀H₄₃O₇P

: 544-97-8
dimethyl zinc(II)

: 944913-72-8
C₂₇H₃₆O₃

: C₂₆H₃₂O₃

Guidance literature:: With CuCN; In tetrahydrofuran; at -15 ℃; for 22h;
DOI:10.1002/anie.200700501

Reference yield:

: 944913-67-1
C₁₇H₂₂O₃

: 944913-72-8
C₂₇H₃₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1: NaI / silver(I) complex of chiral N-heterocyclic carbene; (2-iPrO-3-Ph-C₆H₃)CH=RuCl₂(PPh₃) / tetrahydrofuran / 20 h / -15 °C

2: 70 percent / sodium; ammonia; tBuOH / diethyl ether / 0.05 h / -78 °C

3: imidazole / CH₂Cl₂ / 0.75 h / 22 °C

4: (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂ / benzene / 0.67 h / 22 °C

5: 1.034 g / hydrogen peroxide; KF; KHCO₃ / tetrahydrofuran; methanol; H₂O / 22 °C

6: 96 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 4 h / 22 °C

7: 78 percent / CuCN / tetrahydrofuran / 22 h / -15 °C

With 1H-imidazole; dmap; potassium fluoride; ammonia; dihydrogen peroxide; sodium; potassium hydrogencarbonate; triethylamine; sodium iodide; tert-butyl alcohol; silver(I) complex of chiral N-heterocyclic carbene; (2-iPrO-3-Ph-C₆H₃)CH=RuCl₂(PPh₃); (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; benzene;
DOI:10.1002/anie.200700501

Reference yield:

: 944913-69-3
C₂₅H₃₂O₃

: 944913-72-8
C₂₇H₃₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1: imidazole / CH₂Cl₂ / 0.75 h / 22 °C

2: (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂ / benzene / 0.67 h / 22 °C

3: 1.034 g / hydrogen peroxide; KF; KHCO₃ / tetrahydrofuran; methanol; H₂O / 22 °C

4: 96 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 4 h / 22 °C

5: 78 percent / CuCN / tetrahydrofuran / 22 h / -15 °C

With 1H-imidazole; dmap; potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; triethylamine; (1,3-Mes₂-imidazolidin-2-ylidene)(2-iPrO-benzylidene)RuCl₂; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1002/anie.200700501