(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

Base Information

Chemical Name:(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide
CAS No.:1404287-50-8
Molecular Formula:C₂₇H₃₂ClO₂P
Molecular Weight:454.977
Hs Code.:

Synonyms:(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

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Chemical Property of (4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

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Technology Process of (4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

There total 4 articles about (4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.8%

: 1404287-49-5
(4-hydroxy-3,5-di-tert-butylphenyl)chloromethanediphenylchlorophosphonium chloride

: 149-73-5
trimethyl orthoformate

: 1404287-50-8
(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

Guidance literature:: In benzene; for 0.5h; Reflux;
DOI:10.1134/S1070363214040094

Reference yield: 57.0%

: 1404287-49-5
(4-hydroxy-3,5-di-tert-butylphenyl)chloromethanediphenylchlorophosphonium chloride

: 1404287-50-8
(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

Guidance literature:: With sulfur dioxide; In benzene; for 1h;
DOI:10.1134/S1070363212090241

Reference yield:

: 19382-02-6
4-hydroxy-3,5-di-tert-butylbenzylidene dichloride

: 1404287-50-8
(4-hydroxy-3,5-di-tert-butylphenyl)chloromethyldiphenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hexane / 48 h / 20 °C

2: sulfur dioxide / benzene / 1 h

With sulfur dioxide; In hexane; benzene;
DOI:10.1134/S1070363212090241