3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid

Base Information

• Chemical Name: 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid
• CAS No.: 389602-62-4
• Molecular Formula: C₂₁H₁₄F₃NO₃
• Molecular Weight: 385.342

Synonyms:3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid

Chemical Property of 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid

Chemical Property:

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Technology Process of 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid

There total 1 articles about 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

meta-aminobenzoic acid (99-05-8,159139-79-4) + 4'-trifluoromethylbiphenyl-2-carbonyl chloride (180340-74-3) → 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid (389602-62-4)

Guidance literature:

With N,O-bis-(trimethylsilyl)-acetamide; In water; ethyl acetate;

Reference yield: 95.0%

3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid (389602-62-4) + 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide (68957-94-8) + benzyl-methyl-amine (103-67-3) → N-phenylmethyl-N-methyl-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide (389601-29-0)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane;

Reference yield: 93.0%

(1H-benzo[d]imidazol-5-yl)methanamine + 3-({[4'-(trifluoromethyl)-1,1'-biphenyl-2-yl]carbonyl}amino)benzoic acid (389602-62-4) + 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide (68957-94-8) → N-(1H-Benzimidazol-5-ylmethyl)-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide (389601-65-4)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane;

upstream raw materials:

meta-aminobenzoic acid

4'-trifluoromethylbiphenyl-2-carbonyl chloride

Downstream raw materials:

N-(4-isopropyl-phenylmethyl)-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide

N-(ethoxycarbonylmethyl-aminocarbonylmethyl)-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide

N-(4-methyl-phenylmethyl)-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide

N-phenylmethyl-N-methyl-3-(4'-trifluoromethylbiphenyl-2-carbonylamino)-benzoic acid amide

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