1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

Base Information

• Chemical Name: 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride
• CAS No.: 142062-58-6
• Molecular Formula: C₂₄H₂₈N₂O₃*ClH
• Molecular Weight: 428.959

Synonyms:1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

Chemical Property of 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

Chemical Property:

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Technology Process of 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

There total 6 articles about 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N-<2-(dimethylamino)-6-(3,4,5-trimethoxyphenyl)-3-cyclohexen-1-yl>benzamide (141944-38-9) → 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride (142062-58-6)

Guidance literature:

With trichlorophosphate; for 1.5h; Heating;

DOI:10.1002/jhet.5570290106

Reference yield:

N,N-dimethyl-1,3-butadien-1-amine (139943-10-5,1515-77-1) → 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride (142062-58-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 46 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: 49 percent / glacial acetic acid, Zn / 20 h / Ambient temperature

3: 88 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

4: 53 percent / POCl₃ / 1.5 h / Heating

With sodium hydroxide; acetic acid; hydroquinone; zinc; trichlorophosphate; In chloroform;

DOI:10.1002/jhet.5570290106

Reference yield:

3,4,5-trimethoxy-β-nitrostyrene (6316-70-7) → 1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride (142062-58-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 46 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: 49 percent / glacial acetic acid, Zn / 20 h / Ambient temperature

3: 88 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

4: 53 percent / POCl₃ / 1.5 h / Heating

With sodium hydroxide; acetic acid; hydroquinone; zinc; trichlorophosphate; In chloroform;

DOI:10.1002/jhet.5570290106

upstream raw materials:

N-<2-(dimethylamino)-6-(3,4,5-trimethoxyphenyl)-3-cyclohexen-1-yl>benzamide

N,N-dimethyl-1,3-butadien-1-amine

3,4,5-trimethoxy-β-nitrostyrene

3,4,5-trimethoxy-benzaldehyde

Downstream raw materials:

1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

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