1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

Base Information

• Chemical Name: 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine
• CAS No.: 141944-54-9
• Molecular Formula: C₂₄H₃₀N₂O₃
• Molecular Weight: 394.514

Synonyms:1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

Chemical Property of 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

Chemical Property:

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Technology Process of 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

There total 8 articles about 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride (142062-58-6) → 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine (141944-54-9)

Guidance literature:

With potassium borohydride; In methanol; at 15 - 20 ℃; for 2h;

DOI:10.1002/jhet.5570290106

Reference yield:

N,N-dimethyl-1,3-butadien-1-amine (139943-10-5,1515-77-1) → 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine (141944-54-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 46 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: 49 percent / glacial acetic acid, Zn / 20 h / Ambient temperature

3: benzene / Heating

4: CF₃COOH / 2 h / 73 °C

With acetic acid; hydroquinone; trifluoroacetic acid; zinc; In chloroform; benzene;

DOI:10.1002/jhet.5570290106

Reference yield:

3,4,5-trimethoxy-β-nitrostyrene (6316-70-7) → 1,4,4a,5,6,10b-hexahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine (141944-54-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 46 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: 49 percent / glacial acetic acid, Zn / 20 h / Ambient temperature

3: benzene / Heating

4: CF₃COOH / 2 h / 73 °C

With acetic acid; hydroquinone; trifluoroacetic acid; zinc; In chloroform; benzene;

DOI:10.1002/jhet.5570290106

upstream raw materials:

1,4,4a,10b-tetrahydro-7,8,9-trimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

N,N-dimethyl-1,3-butadien-1-amine

3,4,5-trimethoxy-β-nitrostyrene

3,4,5-trimethoxy-benzaldehyde

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