C₆H₅C₆H₄C₂B₁₀H₁₁

Base Information

• Chemical Name: C₆H₅C₆H₄C₂B₁₀H₁₁
• CAS No.: 885108-79-2
• Molecular Formula: C₁₄H₂₀B₁₀
• Molecular Weight: 296.423
• Mol file: 885108-79-2.mol

Synonyms:C₆H₅C₆H₄C₂B₁₀H₁₁

Chemical Property of C₆H₅C₆H₄C₂B₁₀H₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₅C₆H₄C₂B₁₀H₁₁

There total 1 articles about C₆H₅C₆H₄C₂B₁₀H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-iodo-1,2-dicarba-closo-dodecaborane (137495-63-7) + 2-biphenylmagnesium bromide (82214-69-5) → C6H5C6H4C2B10H11 (885108-79-2)

Guidance literature:

trans-bis(triphenylphosphine)palladium dichloride; In tetrahydrofuran; diethyl ether; addn. of soln. of RMgBr in ether to a soln. of C2B10H11I and (PPh3)2PdCl2 in THF at 0 °C under stirring, heating under reflux for 36 h; addn. of ether, dropwise addn. of water, washing of water layer with ether, washing of combined organic layers with 3% HCl, drying over MgSO4, removal of solvent under vac.;

DOI:10.1016/j.molstruc.2005.10.006

upstream raw materials:

3-iodo-1,2-dicarba-closo-dodecaborane

2-biphenylmagnesium bromide