C₁₅H₁₁Cl₂N

Base Information

Chemical Name:C₁₅H₁₁Cl₂N
CAS No.:957055-23-1
Molecular Formula:C₁₅H₁₁Cl₂N
Molecular Weight:276.165
Hs Code.:

C<sub>15</sub>H<sub>11</sub>Cl<sub>2</sub>N

Synonyms:C₁₅H₁₁Cl₂N

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Chemical Property of C₁₅H₁₁Cl₂N

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Technology Process of C₁₅H₁₁Cl₂N

There total 4 articles about C₁₅H₁₁Cl₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 957055-22-0
C₁₄H₉Cl₂N

: 74-88-4
methyl iodide

: 957055-23-1
C₁₅H₁₁Cl₂N

Guidance literature:: C₁₄H₉Cl₂N; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 2h; Further stages.;
DOI:10.1021/ol701595n

Reference yield:

: 122-78-1
phenylacetaldehyde

: 957055-23-1
C₁₅H₁₁Cl₂N

Guidance literature:: Multi-step reaction with 2 steps

1.1: 78 percent / polyphosphoric acid / tetrahydrofuran / 2 h / Heating

2.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

2.2: 83 percent / tetrahydrofuran / 2 h / 20 °C

With PPA; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ol701595n

Reference yield:

: 608-27-5
2,3-dichloroaniline

: 957055-23-1
C₁₅H₁₁Cl₂N

Guidance literature:: Multi-step reaction with 3 steps

1.1: conc. HCl / methanol

1.2: NaNO₂ / methanol; H₂O / 0.33 h / 0 °C

1.3: 85 percent / SnCl₂*2H₂O; conc. HCl / methanol; H₂O / 6 h / 4 °C

2.1: 78 percent / polyphosphoric acid / tetrahydrofuran / 2 h / Heating

3.1: NaH / tetrahydrofuran / 0.5 h / 20 °C

3.2: 83 percent / tetrahydrofuran / 2 h / 20 °C

With hydrogenchloride; PPA; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1021/ol701595n