Technology Process of 4,5-dichloro-2-nitrophenylazide
There total 7 articles about 4,5-dichloro-2-nitrophenylazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; sodium azide; sodium acetate; sodium nitrite;
Yield given. Multistep reaction;
1.) 0 deg C, 15 min;
DOI:10.1021/jm00010a023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid / 0.25 h / Heating
2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min
3: conc. sulfuric acid / 0.25 h / 100 °C
4: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min
With
hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite;
In
acetic acid;
DOI:10.1021/jm00010a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min
2: conc. sulfuric acid / 0.25 h / 100 °C
3: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min
With
hydrogenchloride; sodium azide; sulfuric acid; nitric acid; sodium acetate; sodium nitrite;
DOI:10.1021/jm00010a023
