trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Base Information

Chemical Name:trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate
CAS No.:1308254-93-4
Molecular Formula:C₁₆H₁₇BN₂O₆S
Molecular Weight:379.174
Hs Code.:

Synonyms:trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

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Chemical Property of trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

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Technology Process of trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

There total 8 articles about trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 811-98-3
d⁽⁴⁾-methanol

: 1308254-89-8
2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetic acid

: 1308254-93-4
trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: sulfuric acid; at 60 ℃;

Reference yield:

: 621-50-1
(3-nitrophenyl)acetonitrile

: 1308254-93-4
trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / methanol / 20 °C

2: hydrogenchloride; iron / water; methanol / 20 °C

3: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C

4: chlorosulfonic acid / 2 h / 0 - 20 °C / Neat (no solvent)

5: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

6: sodium hydroxide; water / methanol / 16 h / 20 °C

7: sulfuric acid / 60 °C

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; chlorosulfonic acid; water; iron; sodium hydroxide; sulfuric acid; In methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 3958-57-4
1-bromomethyl-3-nitrobenzene

: 1308254-93-4
trideuteromethyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1: N,N-dimethyl-formamide / 5 h / 50 °C

2: hydrogenchloride / methanol / 20 °C

3: hydrogenchloride; iron / water; methanol / 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C

5: chlorosulfonic acid / 2 h / 0 - 20 °C / Neat (no solvent)

6: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

7: sodium hydroxide; water / methanol / 16 h / 20 °C

8: sulfuric acid / 60 °C

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; chlorosulfonic acid; water; iron; sodium hydroxide; sulfuric acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;