(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

Base Information

Chemical Name:(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene
CAS No.:1378929-13-5
Molecular Formula:C₆₄H₆₆N₄
Molecular Weight:891.255
Hs Code.:

Synonyms:(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

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Chemical Property of (E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

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Technology Process of (E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

There total 3 articles about (E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4627-22-9
bis(4-tert-butylphenyl)amine

: C₂₄H₁₄Br₂N₂

: 1378929-13-5
(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ruphos; In toluene; at 100 ℃; for 8h; Inert atmosphere;
DOI:10.1002/anie.201108943

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 1378929-13-5
(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate; ruphos / toluene / 8 h / 100 °C / Inert atmosphere

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; ruphos; In tetrahydrofuran; toluene; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1002/anie.201108943

Reference yield:

: 35335-17-2
2,5-bis(diethylphosphonatomethyl)-1,4-dibromobenzene

: 1378929-13-5
(E,E)-2,5-bis[2-(4-cyanophenyl)ethenyl]-1,4-bis[bis(4-tert-butylphenyl)amino]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate; ruphos / toluene / 8 h / 100 °C / Inert atmosphere

With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; ruphos; In tetrahydrofuran; toluene; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1002/anie.201108943