Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester

Base Information

• Chemical Name: Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester
• CAS No.: 79727-58-5
• Molecular Formula: C₂₁H₂₉ClO₃
• Molecular Weight: 364.912

Synonyms:Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester

Chemical Property of Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester

Chemical Property:

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Technology Process of Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester

There total 2 articles about Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propan-1-ol (79727-52-9) + chloroacetyl chloride (79-04-9) → Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester (79727-58-5)

Guidance literature:

In pyridine; Ambient temperature;

DOI:10.1135/cccc19811614

Reference yield:

4-(3,7-dimethyl-2,6-octadienyloxy)propiophenone (37087-78-8) → Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester (79727-58-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

2: 43 percent / pyridine / Ambient temperature

With lithium aluminium tetrahydride; In pyridine; diethyl ether;

DOI:10.1135/cccc19811614

Reference yield: 36.0%

Chloro-acetic acid 1-[4-((E)-3,7-dimethyl-octa-2,6-dienyloxy)-phenyl]-propyl ester (79727-58-5) → Chloro-acetic acid 1-{4-[(E)-5-(3,3-dimethyl-oxiranyl)-3-methyl-pent-2-enyloxy]-phenyl}-propyl ester (79727-73-4)

Guidance literature:

With monoperoxyphthalic acid; In diethyl ether; at 10 - 20 ℃; for 0.5h;

DOI:10.1135/cccc19811614

upstream raw materials:

1-[4-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-phenyl]-propan-1-ol

chloroacetyl chloride

4-(3,7-dimethyl-2,6-octadienyloxy)propiophenone

Downstream raw materials:

Chloro-acetic acid 1-{4-[(E)-5-(3,3-dimethyl-oxiranyl)-3-methyl-pent-2-enyloxy]-phenyl}-propyl ester

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