Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb...

Base Information

• Chemical Name: Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb...
• CAS No.: 103559-38-2
• Molecular Formula: C₉₄H₁₂₅Cl₆N₂O₂₁P
• Molecular Weight: 1862.72
• Mol file: 103559-38-2.mol

Synonyms:Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb...

Chemical Property of Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb...

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Useful:

Technology Process of Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb...

There total 1 articles about Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarbonylamino)-β-D-glucop... (134040-50-9) + chlorophosphoric acid diphenyl ester (2524-64-3) → Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb... (103559-38-2)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 3h; Ambient temperature;

DOI:10.1248/cpb.39.288

Reference yield:

Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-4-O-diphenylphosphono-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarb... (103559-38-2) → C84H115N2O17P

Guidance literature:

With acetic acid; zinc; for 5h; Ambient temperature;

DOI:10.1016/S0040-4039(00)84384-1

upstream raw materials:

Allyl 4-O-benzyl-6-O-<6-O-benzyloxymethyl-3-O-<(R)-3-benzyloxytetradecanoyl>-2-<(R)-3-benzyloxytetradecanoylamino>-2-deoxy-β-D-glucopyranosyl>-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloro-tert-butoxycarbonylamino)-β-D-glucop...

chlorophosphoric acid diphenyl ester