methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

Base Information

Chemical Name:methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate
CAS No.:1365657-16-4
Molecular Formula:C₁₄H₁₇FN₂O₃
Molecular Weight:280.299
Hs Code.:

Synonyms:methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

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Chemical Property of methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

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Technology Process of methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

There total 1 articles about methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365657-20-0
C₇H₁₄N₂O₃

: 459-57-4
4-fluorobenzaldehyde

: 1365657-16-4
methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

Guidance literature:: With magnesium sulfate; In dichloromethane; at 25 ℃;
DOI:10.1016/j.tet.2012.01.100

Reference yield: 56.0%

: 1365657-16-4
methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

: 98-88-4
benzoyl chloride

: 1365657-06-2
5-(dimethylcarbamoyl)-2-(4-fluorophenyl)-1H-pyrrol-3-yl benzoate

Guidance literature:: methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate; With chloro-trimethyl-silane; tetrabutylammonium perchlorate; triethylamine; In tetrahydrofuran; at 25 ℃; Electrochemical reaction;

With hydrogenchloride; In 1,4-dioxane; water; at 25 ℃; for 12h;

benzoyl chloride; With triethylamine; In 1,4-dioxane; at 25 ℃; for 6h;
DOI:10.1016/j.tet.2012.01.100

Reference yield:

: 1365657-16-4
methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate

: 98-88-4
benzoyl chloride

: C₂₀H₁₉FN₂O₃

Guidance literature:: methyl (S,E)-4-(dimethylamino)-3-(4-fluorobenzylideneamino)-4-oxobutanoate; With chloro-trimethyl-silane; tetrabutylammonium perchlorate; triethylamine; In tetrahydrofuran; at 25 ℃; Electrochemical reaction;

benzoyl chloride; With triethylamine; In tetrahydrofuran; at 25 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water; at 25 ℃; for 1h;
DOI:10.1016/j.tet.2012.01.100