1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

Base Information

Chemical Name:1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate
CAS No.:1370528-70-3
Molecular Formula:C₁₃H₁₂F₃NO₄S
Molecular Weight:335.304
Hs Code.:

Synonyms:1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

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Chemical Property of 1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

There total 4 articles about 1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 70571-31-2
1-benzylpiperidine-2,4-dione

: 1370528-70-3
1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tet.2013.04.039

Reference yield:

: 23583-21-3
ethyl-3-benzylamino propionate

: 1370528-70-3
1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: sodium hydride; ethanol / 0 - 20 °C

3: water / acetonitrile / 3.5 h / Reflux

4: triethylamine / dichloromethane / 3 h / 0 - 20 °C

With ethanol; water; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2013.04.039

Reference yield:

: 182559-62-2
ethyl 3-[benzyl(3-ethoxy-3-oxopropyl)amino]-3-oxopropanoate

: 1370528-70-3
1-benzyl-6-oxo-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride; ethanol / 0 - 20 °C

2: water / acetonitrile / 3.5 h / Reflux

3: triethylamine / dichloromethane / 3 h / 0 - 20 °C

With ethanol; water; sodium hydride; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2013.04.039