C₃₄H₄₂O₄Si

Base Information

Chemical Name:C₃₄H₄₂O₄Si
CAS No.:1584730-59-5
Molecular Formula:C₃₄H₄₂O₄Si
Molecular Weight:542.791
Hs Code.:

C<sub>34</sub>H<sub>42</sub>O<sub>4</sub>Si

Synonyms:C₃₄H₄₂O₄Si

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Chemical Property of C₃₄H₄₂O₄Si

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Technology Process of C₃₄H₄₂O₄Si

There total 8 articles about C₃₄H₄₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1584730-47-1
(12S,17S,Z)-12-((tert-butyldiphenylsilyl)oxy)-17-ethyloxacycloheptadeca-10-en-13,15-diyn-2-one

: 1584730-59-5
C₃₄H₄₂O₄Si

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol500667d

Reference yield:

: 1584730-38-0
C₁₈H₃₂O₂Si

: 1584730-59-5
C₃₄H₄₂O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2.1: copper(l) chloride; hydroxylamine hydrochloride; N-butylamine / dichloromethane; water / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 - 20 °C / Inert atmosphere

3.1: Grubbs catalyst first generation / dichloromethane / 12 h / 43 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere

With Grubbs catalyst first generation; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; N-butylamine; 3-chloro-benzenecarboperoxoic acid; copper(l) chloride; In tetrahydrofuran; dichloromethane; water; 2.1: |Cadiot-Chodkiewicz Coupling / 2.2: |Cadiot-Chodkiewicz Coupling;
DOI:10.1021/ol500667d

Reference yield:

: 1584730-42-6
C₃₆H₄₆O₃Si

: 1584730-59-5
C₃₄H₄₂O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / dichloromethane / 12 h / 43 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere

With Grubbs catalyst first generation; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ol500667d