di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

Base Information

Chemical Name:di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate
CAS No.:1610729-02-6
Molecular Formula:C₃₆H₄₄N₈O₆S₂
Molecular Weight:748.927
Hs Code.:

di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

Synonyms:di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

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Chemical Property of di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

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Technology Process of di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

There total 4 articles about di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 897648-31-6
ethyl 2-(4-((tert-butoxycarbonyl)amino)phenyl)acetate

: 1610728-92-1
5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazol-2-amine)

: 1610729-02-6
di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.75h; Microwave irradiation;

Reference yield:

: 1610728-91-0
(S,S)-dibenzyl cyclohexyl 1,3-dicarboxylate

: 1610729-02-6
di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

2: trichlorophosphate / 3 h / 40 - 80 °C

3: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

With palladium 10% on activated carbon; hydrogen; caesium carbonate; trichlorophosphate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 2305-30-8,2305-31-9,3971-31-1,21917-23-7,116724-13-1,116724-14-2
trans-e,a-1,3-cyclohexanedicarboxylic acid

: 1610729-02-6
di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 3 h / 40 - 80 °C

2: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

With caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;