N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

Base Information

Chemical Name:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)
CAS No.:1610728-32-9
Molecular Formula:C₂₆H₂₈N₈O₂S₂
Molecular Weight:548.693
Hs Code.:

Synonyms:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

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Chemical Property of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

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Technology Process of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

There total 5 articles about N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610729-02-6
di-tert-butyl ((((5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(4,1-phenylene))dicarbamate

: 1610728-32-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.5h;

Reference yield:

: 1610728-91-0
(S,S)-dibenzyl cyclohexyl 1,3-dicarboxylate

: 1610728-32-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

2: trichlorophosphate / 3 h / 40 - 80 °C

3: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

4: trifluoroacetic acid / dichloromethane / 0.5 h

With palladium 10% on activated carbon; hydrogen; caesium carbonate; trifluoroacetic acid; trichlorophosphate; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 5438-70-0
ethyl (4-amino-3,5-dibromophenyl)acetate

: 1610728-32-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(4-aminophenyl)acetamide)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 4 h / 85 °C

2: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

3: trifluoroacetic acid / dichloromethane / 0.5 h

With caesium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;