Technology Process of C21H12(2)H3ClF4N4O4
There total 18 articles about C21H12(2)H3ClF4N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
at 50 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 °C
2.1: potassium tert-butylate / N,N-dimethyl acetamide / 0.33 h / 0 - 20 °C
2.2: 100 °C
3.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran; dichloromethane / 20 h / 50 °C
With
potassium tert-butylate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / tetrahydrofuran / 20 h / 20 °C
2.1: potassium tert-butylate / N,N-dimethyl acetamide / 0.33 h / 0 - 20 °C
2.2: 100 °C
3.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran; dichloromethane / 20 h / 50 °C
With
potassium tert-butylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;
