(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

Base Information

Chemical Name:(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid
CAS No.:179082-63-4
Molecular Formula:C₂₉H₃₂N₄O₅
Molecular Weight:516.597
Hs Code.:

Synonyms:(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

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Chemical Property of (R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

Chemical Property:

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Technology Process of (R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

There total 5 articles about (R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13726-84-6,104719-63-3
(tert-butoxy)carbonyl-D-glutamic acid 5-tert-butyl ester

: 179082-63-4
(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / BOP, HOBT, DMAP / dimethylformamide

2: 54 percent / NaH / dimethylformamide

3: 1.) HCl, 2.) Et₃N / 1.) dioxane, 2.) CH₂Cl₂

With hydrogenchloride; dmap; sodium hydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)00062-0

Reference yield:

: 62-53-3
aniline

: 179082-63-4
(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / BOP, HOBT, DMAP / dimethylformamide

2: 54 percent / NaH / dimethylformamide

3: 1.) HCl, 2.) Et₃N / 1.) dioxane, 2.) CH₂Cl₂

With hydrogenchloride; dmap; sodium hydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)00062-0

Reference yield:

: 179083-21-7
(R)-4-tert-Butoxycarbonylamino-4-phenylcarbamoyl-butyric acid tert-butyl ester

: 179082-63-4
(R)-4-[(Isopropyl-phenyl-carbamoylmethyl)-phenyl-carbamoyl]-4-(3-phenyl-ureido)-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / NaH / dimethylformamide

2: 1.) HCl, 2.) Et₃N / 1.) dioxane, 2.) CH₂Cl₂

With hydrogenchloride; sodium hydride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)00062-0