6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one

Base Information

• Chemical Name: 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one
• CAS No.: 1000190-39-5
• Molecular Formula: C₂₈H₂₅N₅O₇
• Molecular Weight: 543.536

Synonyms:6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one

Chemical Property of 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one

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Technology Process of 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one

There total 1 articles about 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)-6-(hydroxymethyl)furo[2,3-d]pyrimidin-2(3H)-one → 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one (1000190-39-5)

Guidance literature:

With diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1055/s-2007-983881

Reference yield: 93.0%

propargyl β-D-2,3,4-O-triacetyl-6-methylglucuronide + 6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one (1000190-39-5) → C44H45N5O17

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 4h;

DOI:10.1055/s-2007-983881

Reference yield: 87.0%

6-(azidomethyl)-3-(2-deoxy-3,5-di-O-4-toluoyl-β-D-ribofuranosyl)furo[2,3-d]pyrimidin-2(3H)-one (1000190-39-5) + 1-O-propargyl 2,3,4,6-tetra-O-acetyl-β-D-glucose (34272-02-1) → C45H47N5O17

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 4h;

DOI:10.1055/s-2007-983881

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