{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

Base Information

Chemical Name:{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide
CAS No.:1181104-55-1
Molecular Formula:C₁₆H₂₅N₂O₆P
Molecular Weight:372.358
Hs Code.:

Synonyms:{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

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Chemical Property of {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

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Technology Process of {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

There total 5 articles about {[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 598-42-5
glycolamide

: 1181104-51-7
methyl hydrogen [(R,S)-1-(benzyloxycarbonylamino)pent-1-yl]phosphonate

: 1181104-55-1
{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tet.2009.05.051

Reference yield:

: 110-62-3
pentanal

: 1181104-55-1
{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / -5 - 20 °C

2.1: sodium hydroxide / methanol; water / 4 h / 80 °C

2.2: pH 1

3.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In methanol; water; acetyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2009.05.051

Reference yield:

: 621-84-1
O-benzyl carbamate

: 1181104-55-1
{[(R,S)-1-benzyloxycarbonylaminopentyl(methoxy)phosphoryl]oxy}acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / -5 - 20 °C

2.1: sodium hydroxide / methanol; water / 4 h / 80 °C

2.2: pH 1

3.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In methanol; water; acetyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2009.05.051