N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine

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Chemical Name:N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine
CAS No.:1101872-56-3
Molecular Formula:C₂₅H₃₅NO₈S
Molecular Weight:509.621
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine

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Chemical Property of N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine

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Technology Process of N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine

There total 2 articles about N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 939985-83-8
tert-butyl N-[2-(2-hydroxy-5-methoxyphenyl)ethyl]-carbamate

: 125562-32-5
2-[2-(benzyloxy)ethoxy]ethyl bromide

: 98-59-9
p-toluenesulfonyl chloride

: 1101872-56-3
N-(tert-butoxycarbonyl)-2-{5-methoxy-2-[2-(2-p-toluenesulfonyloxyethoxy)ethoxy]phenyl}ethylamine

Guidance literature:: tert-butyl N-[2-(2-hydroxy-5-methoxyphenyl)ethyl]-carbamate; 2-[2-(benzyloxy)ethoxy]ethyl bromide; With potassium carbonate; In acetonitrile; at 80 ℃; for 20h;

With 10% Pd/C; hydrogen; In ethanol; at 20 ℃; for 18h;

p-toluenesulfonyl chloride; With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 20h;
DOI:10.1016/j.bmc.2008.10.048