5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

Base Information

Chemical Name:5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate
CAS No.:1388221-48-4
Molecular Formula:C₂₈H₃₁NO₅
Molecular Weight:461.558
Hs Code.:

Synonyms:5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

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Chemical Property of 5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

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Technology Process of 5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

There total 7 articles about 5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201816-71-8
5-(2-hydroxy-4-methoxybenzoyl)-1-o-tolylphenylpyridin-2(1H)-one

: 760-67-8
2-ethylhexanoic acid chloride

: 1388221-48-4
5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2013.06.046

Reference yield:

: 552-41-0
1-(2-hydroxy-4-methoxyphenyl)ethanone

: 1388221-48-4
5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

Guidance literature:: Multi-step reaction with 7 steps

1: sodium / diethyl ether / 0 °C

2: acetic acid; hydrogenchloride / water / 0.5 h / 100 °C

3: methanol / Reflux

4: iodine / dichloromethane

5: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate / water; tetrahydrofuran / 100 °C

6: methanol / Reflux

7: triethylamine / dichloromethane / 1 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; sodium; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; 5: |Heck Reaction;
DOI:10.1016/j.ejmech.2013.06.046

Reference yield:

: 94719-81-0
ω-formyl-4'-methoxy-2'-hydroxyacetophenone

: 1388221-48-4
5-methoxy-2-(6-oxo-1-o-tolyl-1,6-dihydropyridine-3-carbonyl)phenyl 2-ethylhexanoate

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid; hydrogenchloride / water / 0.5 h / 100 °C

2: methanol / Reflux

3: iodine / dichloromethane

4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate / water; tetrahydrofuran / 100 °C

5: methanol / Reflux

6: triethylamine / dichloromethane / 1 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 4: |Heck Reaction;
DOI:10.1016/j.ejmech.2013.06.046