N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

Base Information

Chemical Name:N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide
CAS No.:1445890-40-3
Molecular Formula:C₃₁H₄₄ClN₇O₃Si₂
Molecular Weight:654.359
Hs Code.:

N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

Synonyms:N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

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Chemical Property of N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

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Technology Process of N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

There total 1 articles about N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: [1-(trimethylsilyl)ethoxy]methyl chloride

: 1445888-28-7
N-{4-[3-(2-chlorophenyl)-4-(4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}acetamide

: 1445890-40-3
N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

Guidance literature:: N-{4-[3-(2-chlorophenyl)-4-(4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}acetamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.0833333h; Inert atmosphere;

[1-(trimethylsilyl)ethoxy]methyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 24h;

Reference yield: 82.0%

: 1445890-40-3
N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

: 1445890-42-5
4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-amine

Guidance literature:: With water; sodium hydroxide; In ethanol; for 2h; Reflux;

Reference yield:

: 1445890-40-3
N-{4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}-N-{[2-(trimethylsilyl)ethoxy]methyl}acetamide

: 1445890-44-7
methyl {4-[3-(2-chlorophenyl)-4-(4-{[2-(trimethylsilyl)ethoxy]methyl}-4H-1,2,4-triazol-3-yl)-1H-pyrazol-1-yl]-5-methylpyridin-2-yl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol / 2 h / Reflux

2: triethylamine / dichloromethane / 6 h / 20 °C

With water; triethylamine; sodium hydroxide; In ethanol; dichloromethane;