(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

Base Information

Chemical Name:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate
CAS No.:1335107-39-5
Molecular Formula:C₁₄H₁₇F₃O₅S
Molecular Weight:354.347
Hs Code.:

Synonyms:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

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Technology Process of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

There total 1 articles about (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 351003-43-5
3,4,5-trifluorobenzene-1-sulfonyl chloride

: 3663-46-5
5-hydroxymethyl-2,2,5-trimethyl-1,3-dioxane

: 1335107-39-5
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja207004v

Reference yield: 75.0%

: 1335107-39-5
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

: 1335107-42-0
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,5-difluoro-4-hydrazinylbenzenesulfonate

Guidance literature:: With potassium carbonate; hydrazine hydrate; In acetonitrile; at 20 ℃;
DOI:10.1021/ja207004v

Reference yield:

: 1335107-39-5
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4,5-trifluorobenzenesulfonate

: 1335107-45-3
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 4-(3-(4-cyanophenyl)-5-(4-(3,3,13,13-tetramethyl-2,4,12,14-tetraoxa-8,17,23-trithia-20-azadispiro[5.3.5.9]tetracosan-20-yl)phenyl)-4,5-dihydro-1H-pyrazol-1-yl)-3,5-difluorobenzene-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; hydrazine hydrate / acetonitrile / 20 °C

2: pyridine; pyridinium p-toluenesulfonate / 24 h / 90 - 100 °C / Inert atmosphere

With pyridine; pyridinium p-toluenesulfonate; potassium carbonate; hydrazine hydrate; In acetonitrile;
DOI:10.1021/ja207004v