Technology Process of potassium 3,5-bis-(trifluoromethyl)benzoyltrifluoroborate
There total 1 articles about potassium 3,5-bis-(trifluoromethyl)benzoyltrifluoroborate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3,6-bis(trifluoromethyl)bromobenzene; (ethylthiotrifluoroborate)methane dimethyliminium zwitterion;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
Inert atmosphere;
With
acetone;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.166667h;
Inert atmosphere;
potassium fluoride;
In
tetrahydrofuran; hexane; water;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1002/anie.201403931
