Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

Base Information

Chemical Name:Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine
CAS No.:372107-44-3
Molecular Formula:C₂₂H₁₈N₄
Molecular Weight:338.412
Hs Code.:

Synonyms:Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

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Technology Process of Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

There total 1 articles about Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 36640-50-3
1-phenyl-3-(pyridin-3-yl)-1H-pyrazole-4-carboxaldehyde

: 100-46-9
benzylamine

: 372107-44-3
Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

Guidance literature:: In acetic acid; toluene; for 1h; Heating;
DOI:10.1007/s11178-005-0128-8

Reference yield: 73.0%

: 372107-44-3
Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

: benzyl-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-ylmethyl)-amine; hydrochloride

Guidance literature:: Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine; With sodium tetrahydroborate; In methanol; ethanol; at 20 ℃; for 3h;

With hydrogenchloride;
DOI:10.1007/s11178-005-0128-8

Reference yield:

: 372107-44-3
Benzyl-[1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-yl)-meth-(E)-ylidene]-amine

: 1-benzyl-3-phenyl-1-(1-phenyl-3-pyridin-3-yl-1H-pyrazol-4-ylmethyl)-thiourea

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydridoborate / methanol; ethanol / 3 h / 20 °C

1.2: 73 percent / HCl

2.1: 65 percent / triethylamine / ethanol / 1 h / Heating

With sodium tetrahydroborate; triethylamine; In methanol; ethanol;
DOI:10.1007/s11178-005-0128-8