1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

Base Information

Chemical Name:1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime
CAS No.:902772-61-6
Molecular Formula:C₂₄H₁₉ClN₄O₇
Molecular Weight:510.89
Hs Code.:

Synonyms:1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

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Technology Process of 1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

There total 3 articles about 1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 902772-55-8
1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone oxime

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 902772-61-6
1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

Guidance literature:: With sodium ethanolate; In ethanol; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2006.04.041

Reference yield:

: 902772-53-6
1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone

: 902772-61-6
1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / hydroxylamine hydrochloride; potassium hydroxide / aq. ethanol / 45 h / Heating

2: 64 percent / NaOEt / ethanol / 0.5 h / 20 °C

With potassium hydroxide; hydroxylamine hydrochloride; sodium ethanolate; In ethanol;
DOI:10.1016/j.tet.2006.04.041

Reference yield:

: 151290-21-0
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole

: 902772-61-6
1-[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-yl]ethanone O-(2,4-dinitrophenyl)oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoryl chloride / 50 - 60 °C

1.2: 52 percent / sodium hydroxide / H₂O / 3 h / 20 °C / pH 14

2.1: 80 percent / hydroxylamine hydrochloride; potassium hydroxide / aq. ethanol / 45 h / Heating

3.1: 64 percent / NaOEt / ethanol / 0.5 h / 20 °C

With potassium hydroxide; hydroxylamine hydrochloride; sodium ethanolate; trichlorophosphate; In ethanol;
DOI:10.1016/j.tet.2006.04.041