3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

Base Information

Chemical Name:3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside
CAS No.:937023-68-2
Molecular Formula:C₇₁H₁₀₈O₉
Molecular Weight:1105.63
Hs Code.:

Synonyms:3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

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Chemical Property of 3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

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Technology Process of 3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

There total 5 articles about 3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 937023-67-1
3-benzyloxy-2,2-dihexadecyloxymethyl-1,3-propanol

: 159407-17-7
phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 937023-68-2
3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

: 3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-α-D-mannopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; 1-benzenesulfinyl piperidine; trifluoromethanesulfonic acid anhydride; In dichloromethane; at -78 - 0 ℃;
DOI:10.1016/j.tetlet.2007.02.086

Reference yield:

: 937023-66-0
3,3-dihexadecyloxymethyl-1,5-dioxaspiro[5.5]undecan

: 937023-68-2
3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / neopentyl glycol; camphorsulfonic acid / CH₂Cl₂ / 35 °C

2.1: Bu₂SnO / benzene / 90 °C

2.2: 70 percent / tetrabutylammonium bromide / 90 °C

3.1: 85 percent / 1-benzenesulfinyl piperidine; trifluoromethanesulfonic anhydride; 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / -78 - 0 °C

With 2,6-di-tert-butyl-4-methylpyridine; 1-benzenesulfinyl piperidine; camphor-10-sulfonic acid; di(n-butyl)tin oxide; trifluoromethanesulfonic acid anhydride; 2,2-Dimethyl-1,3-propanediol; In dichloromethane; benzene;
DOI:10.1016/j.tetlet.2007.02.086

Reference yield:

: 714-88-5
Cyclohexanone cyclic 2,2-bis(hydroxymethyl)trimethylene ketal

: 937023-68-2
3-benzyloxy-2,2-dihexadecyloxymethylpropyl 2,3-di-O-benzyl-4,6-di-O-benzylidene-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 59 percent / NaH / dimethylformamide / 50 °C

2.1: 95 percent / neopentyl glycol; camphorsulfonic acid / CH₂Cl₂ / 35 °C

3.1: Bu₂SnO / benzene / 90 °C

3.2: 70 percent / tetrabutylammonium bromide / 90 °C

4.1: 85 percent / 1-benzenesulfinyl piperidine; trifluoromethanesulfonic anhydride; 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / -78 - 0 °C

With 2,6-di-tert-butyl-4-methylpyridine; 1-benzenesulfinyl piperidine; camphor-10-sulfonic acid; sodium hydride; di(n-butyl)tin oxide; trifluoromethanesulfonic acid anhydride; 2,2-Dimethyl-1,3-propanediol; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2007.02.086