Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

Base Information

Chemical Name:Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide
CAS No.:424823-29-0
Molecular Formula:C₇₁H₁₁₈N₂O₈
Molecular Weight:1127.73
Hs Code.:

Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

Synonyms:Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

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Technology Process of Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

There total 7 articles about Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 424823-30-3
(2S,3S,4R)-2-hexacosanoylamido-(2,3,4-tri-O-benzyl-6-deoxy-6-azido-α-D-galactopyranosyloxy)octadecane-3,4-diol

: 424823-29-0
Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1021/ol025565+

Reference yield:

: 1-O-acetyl-6-azido-2,3,4-tri-O-benzyl-6-deoxy-α,β-D-galactopyranose

: 424823-29-0
Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / HF*pyridine / pyridine; toluene / 6 h / 0 °C

2: 44 percent / molecular sieves 4 Angstroem; AgClO₄; SnCl₂ / tetrahydrofuran / 2 h / 0 - 20 °C

3: 81 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

4: 99 percent / PPh₃ / tetrahydrofuran; H₂O / 12 h / 20 °C

With 4 A molecular sieve; tetrabutyl ammonium fluoride; silver perchlorate; pyridine hydrogenfluoride; triphenylphosphine; tin(ll) chloride; In tetrahydrofuran; pyridine; water; toluene;
DOI:10.1021/ol025565+

Reference yield:

: 205371-68-2
(2S,3S,4R)-3,4-di-O-tertbutyldimethylsilyl-2-(N-hexacosanoylamino)octadecan-1,3,4-triol

: 424823-29-0
Hexacosanoic acid [(1S,2S,3R)-1-((2S,3R,4S,5S,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxymethyl)-2,3-dihydroxy-heptadecyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 44 percent / molecular sieves 4 Angstroem; AgClO₄; SnCl₂ / tetrahydrofuran / 2 h / 0 - 20 °C

2: 81 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

3: 99 percent / PPh₃ / tetrahydrofuran; H₂O / 12 h / 20 °C

With 4 A molecular sieve; tetrabutyl ammonium fluoride; silver perchlorate; triphenylphosphine; tin(ll) chloride; In tetrahydrofuran; water;
DOI:10.1021/ol025565+