3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

Base Information

Chemical Name:3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide
CAS No.:122689-94-5
Molecular Formula:C₃₀H₂₆N₂OS
Molecular Weight:462.615
Hs Code.:

Synonyms:3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

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Chemical Property of 3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

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Technology Process of 3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

There total 6 articles about 3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 122689-86-5
Dibenzyl-(3-phenyl-4-phenylsulfanylmethyl-isoxazol-5-yl)-amine

: 122689-94-5
3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

Guidance literature:: In neat (no solvent); at 175 ℃; for 0.2h;
DOI:10.1016/S0040-4039(00)82266-2

Reference yield:

: 29278-09-9
5-amino-3-phenyl-isoxazole-4-carboxylic acid ethyl ester

: 122689-94-5
3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / dimethylformamide / 0 - 25 °C

2: LAH / tetrahydrofuran / 0 - 25 °C

3: pyridine

4: dimethylformamide / 0 °C

5: 70 percent / neat (no solvent) / 0.2 h / 175 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)82266-2

Reference yield:

: 100-39-0
benzyl bromide

: 122689-94-5
3-Phenyl-2-phenylsulfanylmethyl-2H-azirine-2-carboxylic acid dibenzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / dimethylformamide / 0 - 25 °C

2: LAH / tetrahydrofuran / 0 - 25 °C

3: pyridine

4: dimethylformamide / 0 °C

5: 70 percent / neat (no solvent) / 0.2 h / 175 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)82266-2