[(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

Base Information

Chemical Name:[(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate
CAS No.:905581-46-6
Molecular Formula:C₄₁H₃₆N₆O₈S
Molecular Weight:772.838
Hs Code.:

[(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

Synonyms:[(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

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Chemical Property of [(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

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Technology Process of [(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

There total 1 articles about [(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 905581-37-5
((3aR,4R,6R,6aR)-6-(6-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro-[3,4-d][1,3]dioxol-4-yl)methyl tritylsulfamate

: 905581-46-6
[(3aR,4R,6R,6aR)-6-{6-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-methyl]-9H-purine-9-yl}-2,2-dimethyltetrahyrofuro[3,4-d][1,3]dioxol-4-yl]-methyl tritylsulfamate

Guidance literature:: N-(bromomethyl)phtalimide; With chloro-trimethyl-silane; ethylene dibromide; zinc; In N,N-dimethyl-formamide; at 0 - 20 ℃;

((3aR,4R,6R,6aR)-6-(6-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro-[3,4-d][1,3]dioxol-4-yl)methyl tritylsulfamate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; for 48h;