5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

Base Information

Chemical Name:5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester
CAS No.:115840-23-8
Molecular Formula:C₁₃H₁₅ClFNO₄
Molecular Weight:303.718
Hs Code.:

Synonyms:5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

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Chemical Property of 5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

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Technology Process of 5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

There total 3 articles about 5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134605-95-1
2-chloro-4-fluoro-5-nitrobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

: 115840-23-8
5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

Guidance literature:: With hydrogenchloride; In ethanol; water;

Reference yield:

: 80-55-7
ethyl 2-hydroxy-2,2-dimethylethanoate

: 115840-23-8
5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol / 2 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;

Reference yield:

: 114776-15-7
2-chloro-4-fluoro-5-nitrobenzoic acid

: 115840-23-8
5-amino-2-chloro-4-fluorobenzoic acid(1-methyl-1-ethoxycarbonyl)ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol / 2 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;