triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

Base Information

Chemical Name:triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate
CAS No.:1048642-06-3
Molecular Formula:C₁₃H₁₇F₂O₅S*C₁₈H₁₅S
Molecular Weight:586.721
Hs Code.:

Synonyms:triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

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Chemical Property of triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

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Technology Process of triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

There total 5 articles about triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1048642-04-1
adamantane-1-carboxylic acid 2,2-difluoro-2-methanesulfonylethyl ester sodium salt

: 1048642-06-3
triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

Guidance literature:: With triphenylsulfonium chloride; In water; at 20 ℃; for 1.5h;

Reference yield:

: 1048642-04-1
adamantane-1-carboxylic acid 2,2-difluoro-2-methanesulfonylethyl ester sodium salt

: 4270-70-6
triphenylsulfonium chloride

: 1048642-06-3
triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

Guidance literature:: In water; at 20 ℃; for 1.5h;

Reference yield:

: 1048642-02-9
(2'-bromo-2',2'-difluoro)ethyl 1-adamantanecarboxylate

: 1048642-06-3
triphenylsulfonium 2-(1'-adamantane)carbonyloxy-1,1-difluoroethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate; sodium dithionite / acetonitrile; water / 90 h / 70 - 80 °C / Inert atmosphere

2: dihydrogen peroxide; sodium tungstate (VI) dihydrate / water / 2 h / 20 °C

3: triphenylsulfonium chloride / water / 1.5 h / 20 °C

With sodium dithionite; sodium tungstate (VI) dihydrate; dihydrogen peroxide; triphenylsulfonium chloride; sodium hydrogencarbonate; In water; acetonitrile;