(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

Base Information

Chemical Name:(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate
CAS No.:702711-15-7
Molecular Formula:C₃₃H₃₅NO₄SeSi
Molecular Weight:616.691
Hs Code.:

Synonyms:(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

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Technology Process of (1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

There total 1 articles about (1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4461-33-0
benzoyl isocyanate

: 702711-07-7
(2R)-1-{[tert-butyl(diphenyl)silyl]oxy}-3-(phenylseleno)propan-2-ol

: 702711-15-7
(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1002/chem.200305497

Reference yield:

: 702711-15-7
(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

: C₃₃H₃₅NO₅SeSi

Guidance literature:: With dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; for 2h;
DOI:10.1002/chem.200305497

Reference yield:

: 702711-15-7
(1R)-2-[(tert-butyl(diphenyl)silyl)oxy]-1-[(phenylseleno)methyl]ethylbenzoylcarbamate

: 702711-16-8
(5S)-3-benzoyl-5-{[(tert-butyl(diphenyl)silyl)oxy]methyl}-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogenphosphate; m-chloroperoxybenzoic acid / tetrahydrofuran / 2 h

2: K₂CO₃ / acetone / 20 °C

With dipotassium hydrogenphosphate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; acetone;
DOI:10.1002/chem.200305497